Methyl Orange 0.1 Percent (w/v) Aqueous Indicator Solution (U.S.P. Test Solution) Ion-Catalyzed Organic Synthesis ANHYDROUS BASIS) 19 23% NICOTINE

ANHYDROUS BASIS) 19 23% NICOTINE RELEASE 70 % of total 70 % of total WATER DETERMINATION 5

/td> WATER DETERMINATION 0

00% MICROBIAL LIMITS: ESCHERICHIA COLI NEGATIVE SALMONELLA NEGATIVE IDENTIFICATION TO PASS TEST TO PASS TEST EXPIRATION DATE

5 IRON (Fe) 80 ppm MICROBIAL CONTAMINATION (TAMC) 100 CFU/g APPEARANCE OF SOLUTION TO PASS TEST TO PASS TEST ELEMENTAL IMPURITIES AS REPORTED AS REPORTED IDENTIFICATION TO PASS TEST TO PASS TEST RETEST DATE MANUFACTURE DATE APPEARANCE RESIDUAL SOLVENTS TO PASS TEST TO PASS TEST

0 % WATER 3

Methyl Orange 0.1 Percent (w/v) Aqueous Indicator Solution (U.S.P. Test Solution) Ion-Catalyzed Organic Synthesis ANHYDROUS BASIS) 19 23% NICOTINETest Specification Min Max SUITABILITY AS AN INDICATOR PASSES TEST PASSES TEST EXPIRATION DATE