Ketoconazole Detection of Amines for Primary Amines (for Detection of Free Amine on the Resins) Test Specification Min Max SAPONIFICATION

Test Specification Min Max SAPONIFICATION VALUE 57 - 64 57 - 64 ACID VALUE 2 MOISTURE 3

00% HEAVY METALS (by ICP-OES) 5 ppm IRON (Fe) 2 ppm

02% ARSENIC (As) 1 ppm COPPER (Cu) 0

0 COLOR (APHA) 150 POLYETHYLENE GLYCOL 4

00% PARTICLE SIZE DISTRIBUTION (Over size) 10

Ketoconazole Detection of Amines for Primary Amines (for Detection of Free Amine on the Resins) Test Specification Min Max SAPONIFICATIONTest Specification Min Max ASSAY (DRIED BASIS) 98. 0 102. 0 % 98. 0 102. 0 % MELTING RANGE 148 152C 148 152C SPECIFIC ROTATION, [a][@D@]20 1 to +1 1 to +1 CHROMATOGRAPHIC PURITY TO PASS TEST TO PASS TEST LOSS ON DRYING 0. 50% RESIDUE ON IGNITION 0. 10% HEAVY METALS 0. 00%