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10.1021/tx060142s 39 KonK.KimJ.-S.JaeschkeH.LemastersJ
Complete, the reaction solution was concentrated, the concentration was completed, the residue 1378ml isopropyl ether was slurried at room temperature, filtered, 564ml of acetonitrile was added to the filter cake, slurried at room temperature, and dried to obtain 36.13g white solid powder terminal dipeptide fragment, purity 98.27%, yield 70.50 %, the isomer content is 0.05%