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Pituitary Adenylate Cyclase-Activating Polypeptide Pituitary adenylate cyclase-activating polypeptide (PACAP) is very rapidly degraded by DPP4 to the fragments (327), (527), and (627)

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The cis-piperidinone was epimerized to the required trans isomer using a base-catalyzed, dynamic crystallization-driven procedure, which was subsequently crystallized from the raw reaction mixture with high yield and purity