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The eluate was further purified using SEC (Superose 6 increase 100/30 Cytiva) with the SEC buffer (20 mM Hepes pH7.5 and 400 mM NaCl)

Compounds were annotated by matching to LCMS method-specific retention time values of external standards and MS 2 spectral matching to external standards and the mzCloud database (Thermo Scientific)

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